Bubble (Air-leak) Testing

A. Introduction 

DestructiveTo detect microleaks in hermetically sealed packages by visually inspecting for gas bubbles escaping through the leaks due to the pressure differential.> 20 μm pinhole, > 50 μm microchannelOff-line, > 30 sec/test$5,000-15,000

B. Operation 

Bubble testing is the simplest, least expensive method of detecting and assessing leaks. The procedure involves creation of a pressure differential across the package with air (or some other gas) on the high pressure side (inside package) and a water chamber on the low pressure side (outside package). Leak detection is performed by immersing the package in a water-filled test chamber. The headspace above the water level is evacuated, which cause the package to inflate. If there's a leak, air or gas flow through leaks will result in the formation of bubbles outside the package. This method provides immediate indications of the existence and location of small leaks.

Disadvantages include a long test time (a minimum of 30 seconds per test), low sensitivity, the tendency of leaks to get clogged by viscous food materials during testing, water contamination, and part clean-up time. The sensitivity of the test is not high, due to operator dependence. The reproducibility and sensitivity of bubble testing depends on the use of a dark background (increased contrast), high pressure differentials, and the operator.

  • Vacuum water chamber with a regulator
  • Vaucum pump
  • Water
  1. Fill the chamber with enough water to submerge a package when expanded.
  2. Place a package to be tested in the chamber and close the lid.
  3. Turn on a vacuum pump and open a regulator valve to generate vacuum inside. 
  4. Increase vacuum (up to 30 inHg) until the package is expanded. Bubbles will rise from a leak.
  5. When testing is complete, switch off pump and relieve the vacuum.

Positive

A steady stream of bubbles comes from the package at one or more locations.

Negative

No bubbles are emitted from the package.

False Positive

Bubbles cling to surface of the package after package is submerged in water.

False Negative

Food particles block holes through which air might escape from defective package; or vacuum used is insufficient to force air through minute holes in package.

C. Application 

PACKAGE TYPES AND DEFECTS

 PACKAGE TYPE
DEFECTSFlexible PouchSemi-rigid and
Rigid plastic container
Plastic Can (Double-seam Metal End)Paperboard
Abrasion
Corner Dent   
Crushed 
Cut (Fracture)
Delamination 
Double Seam Defects*   
Flexcracks 
Foreign Matter Inclusion  
Gels  
Hotfold   
Label Foldover   
Leaker   
Leaker (Channel) 
Leaker (Corner)   
Leaker (Notch)   
Leaker (Perforation)   
Leaker (Pulltab)   
Leaker (Seal)   
Loose Flap or Ear   
Malformed  
Puncture (Pinhole)
Seal Defects (Blister)   
Seal Defects (Blocked)   
Seal Defects (Burnt)   
Seal Defects (Compressed)   
Seal Defects (Contaminated)  
Seal Defects (Convolution/Embossing)   
Seal Defects (Creep)   
Seal Defects (Crooked)   
Seal Defects (Incomplete)   
Seal Defects (Misaligned/Deformed)  
Seal Defects (Nonbonding/Weak)   
Seal Defects (Plastic Lumps)   
Seal Defects (Seal-width Variation)   
Seal Defects (Stringy)   
Seal Defects (Uneven Impression)   
Seal Defects (Uneven Juncture)   
Seal Defects (Wrinkle)  
Swell (Swollen Package)
Waffling   

D. Source 

  • Haug Quality Equipment, 18443 Technology Drive, Morgan Hill, CA 95037. TEL (408)-465-8160 (http://www.haugquality.com/index.html)Flex Essentials Inc. 17769 Centreville Creek Road, Caledon East, Ontario, L7K 2L9 Canada. TEL (416) 399-5583 (http://www.flexpakinc.com )ASTM D3078 - 02(2008) Standard Test Method for Determination of Leaks in Flexible Packaging by Bubble Emission
  • Floros, J.D. and Gnanasekharan, V. 1992. Principles, technology and applications of destructive and nondestructive package integrity testing. In Advances in Aseptic Processing Technologies, Singh, R.K. and Nelson, P.E. (Eds), pp. 157-188, Elsevier Sci. Publ. Ltd., New York, NY.